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β,β′-Phenylene bridged hexaphyrin[1.0.1.0.1.0] (naphthorosarin), an expanded porphyrin possessing C 3v -symmetry, has been shown to possess unique electronic features. We now report a bimetallic Rh( i )-complex of naphthorosarin retaining 24 π-antiaromatic characteristics. The two Rh( i ) cations reside on opposite sides of the macrocyclic π-system and are separated at a distance consistent with a possible Rh( i )–Rh( i ) metallic bond interaction.more » « less